CAS 5720-06-9 | 2-Methoxyphenylboronic Acid

Molecular Formula: C7H9BO3
Molecular Weight: 151.96
EINECS: 611-481-7
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Application

Specification of CAS 5720-06-9 | 2-Methoxyphenylboronic acid

ITEMS

SPECIFICATION

Melting point

105-110 °C (lit.)

InChIKey

ROEQGIFOWRQYHD-UHFFFAOYSA-N

Storage temp.

Keep in dark place,Sealed in dry,Room Temperature

Color

Off-white

Form

Crystals or Crystalline Powder

Water Solubility

Insoluble in water.

Density

1.17 g/cm3

Boiling point

319.3 °C

pka

8.55

BRN

3030981

CAS DataBase Reference

5720-06-9(CAS DataBase Reference)

Synthesis of CAS 5720-06-9 | 2-Methoxyphenylboronic acid

CAS 5720-06-9 | 2-Methoxyphenylboronic Acid

Conditions

Stage #1: 2-bromoanisole With n-butyllithium In diethyl ether; hexane at -78 – 20℃; Inert atmosphere;

Stage #2: Trimethyl borate In diethyl ether; hexane at -78 – 20℃; Inert atmosphere; Stage #3: With hydrogenchloride In diethyl ether; hexane; water for 1h;

Reference

Sweetman, Brian A.; Guiry, Patrick J.

[Tetrahedron, 2018, vol. 74, # 38, p. 5567 – 5581]


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