CAS 644-36-0 | 2-Methylphenylacetic Acid

Molecular Formula: C9H10O2
Molecular Weight: 150.17
EINECS: 211-416-9
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
Worldwide Delivery

Application

Specification of CAS 644-36-0 | 2-Methylphenylacetic acid

ITEMS

SPECIFICATION

Melting point

88-90 °C (lit.)

InChIKey

RZWGTXHSYZGXKF-UHFFFAOYSA-N

Storage temp.

Sealed in dry,Room Temperature

Color

White to slightly cream

Refractive index

1.5470

Form

Crystalline Powder

Water Solubility

insoluble

Density

0.9820

Boiling point

211.72°C

pka

pK1

NIST Chemistry Reference

O-tolylacetic acid(644-36-0)

BRN

1936952

CAS DataBase Reference

644-36-0(CAS DataBase Reference)


Synthesis of CAS 644-36-0 | 2-Methylphenylacetic acid

CAS 644-36-0 | 2-Methylphenylacetic Acid

Conditions

Stage #1: carbon monoxide With C28H22CoN4O6 In butan-1-ol at 60℃; under 760.051 Torr; for 2h; Glovebox; High pressure; Green chemistry;

Stage #2: 1-chloromethyl-2-methylbenzene With tetra-(n-butyl)ammonium iodide; sodium hydroxide In butan-1-ol at 60℃; under 760.051 Torr; for 22h; Glovebox; High pressure; Green chemistry; regioselective reaction;


Reference

She, Meng-Yao; Xiao, Da-Wei; Yin, Bing; Yang, Zheng; Liu, Ping; Li, Jian-Li; Shi, Zhen

[Tetrahedron, 2013, vol. 69, # 35, p. 7264 – 7268]

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