CAS 709031-45-8 | Saxagliptin Intermediate

Molecular Formula: C7H14N2O4S
Molecular Weight: 222.26
EINECS: 615-206-1
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg

Application

Introduction
(1S,3S,5S)-2-Azabicyclo[3.1.0]hexane-3-carboxamide MonoMethanesulfonate is a saxagliptin intermediate.

Specification of CAS 709031-45-8 | 2-Azabicyclo[3.1.0]hexane-3-carboxaMide, (1S,3S,5S)-,MonoMethanesulfonate

ITEMS

SPECIFICATION

storage temp.

Inert atmosphere,Room Temperature

Synthesis of CAS 709031-45-8 | 2-Azabicyclo[3.1.0]hexane-3-carboxaMide, (1S,3S,5S)-,MonoMethanesulfonate

CAS 709031-45-8 | Saxagliptin Intermediate


Conditions:

In isopropyl alcohol at 55 – 65℃; for 3.5h; Large scale reaction;


Reference:

Savage, Scott A.; Jones, Gregory S.; Kolotuchin, Sergei; Ramrattan, Shelly Ann; Vu, Truc; Waltermire, Robert E.

[Organic Process Research and Development, 2009, vol. 13, # 6, p. 1169 – 1176]

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